Lift mode
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The use of AFM for examination of magnetic and electric structures
is known practically since the invention of this technique. Initially,
the probes made of ferromagnetic and conducting materials were employed
for detection of surface magnetic and electric features, respectively.
The forces between these objects were detected through response
of oscillating probes placed close to the samples but operating
in the non-contact mode. These measurements have also revealed a
need in separation of effects caused by magnetic and electrostatic
interactions from those caused by van der Waals forces. The situation
is even more complicated when magnetic or electric studies are performed
in the tapping mode. This problem has been partially solved with
introduction of the so-called lift mode.
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| (a) Height image obtained in Tapping mode. |
(b) EFM map (phase image) of the same area.
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| Height and phase images of the rubber-modified
isotactic polypropylene filled with carbon black. The images were
obtained in Electric Force Microscopy mode using NSC14 probes coated
with Pt: the height image was obtained in the first pass and the phase
image was obtained in the second pass with the lift of 20 nm. Images
courtesy of S. Magonov. |
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The lift mode or a two-pass technique is used in magnetic force
microscopy (MFM) and electric force microscopy (EFM) to separate
the effects of the electric and mechanical forces tip-sample forces.
For each scan line, the height profile is recorded during the first
pass. At the end of the first pass the probe is lifted typically
5-50 nanometers above the surface. Then it is moved along the just-learned
height contour at a constant lift height (typically 10-50 nm). During
this second pass, the changes of the probe resonant frequency or
the phase, which are caused by the long-distant magnetic or electric
forces, are monitored. In this way the height image is recorded
in the first pass and the frequency (phase) image recorded in the
second pass. To some extent, this approach allows to separate the
topographic and magnetic (electric) effects. However, the two-pass
technique required twice more time for imaging. There are also other
disadvantages, for example, a remote position of the probe during
the second pass, which reduces a resolution and sensitivity of electric
and magnetic imaging.
In past several years the interest to AFM-related modes for probing
of electric and magnetic properties has increased due to improvements
in EFM and Kelvin Force Microscopy. Kelvin Force Microscopy is method
closely related to EFM but it provides quantitative measurements
of surface potential. This is achieved by using an additional feedback
mechanism, in which a voltage applied to the probe nullifies the
effect of the contact potential difference (between the probe and
the sample) on the oscillating probe. (In the tapping mode operation
the KFM measurements are also can be done in the lift mode) In this
way surface potential or surface charge can be measured quantitatively.
The increasing use of several lock-in amplifiers in the home-made
and commercial scanning probe microscope allows researchers to perform
topographic and electrostatic measurements in the single scan by
operating the related signals and feedback loops at different frequencies.
This approach has definite advantages compared to the two-pass mode:
the improved sensitivity, higher resolution and a reduced experiment
time.
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