How To Choose   by AFM Techniques  

Lift mode

Options

The use of AFM for examination of magnetic and electric structures is known practically since the invention of this technique. Initially, the probes made of ferromagnetic and conducting materials were employed for detection of surface magnetic and electric features, respectively. The forces between these objects were detected through response of oscillating probes placed close to the samples but operating in the non-contact mode. These measurements have also revealed a need in separation of effects caused by magnetic and electrostatic interactions from those caused by van der Waals forces. The situation is even more complicated when magnetic or electric studies are performed in the tapping mode. This problem has been partially solved with introduction of the so-called lift mode.

(a) Height image obtained in Tapping mode. (b) EFM map (phase image) of the same area.  
Height and phase images of the rubber-modified isotactic polypropylene filled with carbon black. The images were obtained in Electric Force Microscopy mode using NSC14 probes coated with Pt: the height image was obtained in the first pass and the phase image was obtained in the second pass with the lift of 20 nm. Images courtesy of S. Magonov.

The lift mode or a two-pass technique is used in magnetic force microscopy (MFM) and electric force microscopy (EFM) to separate the effects of the electric and mechanical forces tip-sample forces. For each scan line, the height profile is recorded during the first pass. At the end of the first pass the probe is lifted typically 5-50 nanometers above the surface. Then it is moved along the just-learned height contour at a constant lift height (typically 10-50 nm). During this second pass, the changes of the probe resonant frequency or the phase, which are caused by the long-distant magnetic or electric forces, are monitored. In this way the height image is recorded in the first pass and the frequency (phase) image recorded in the second pass. To some extent, this approach allows to separate the topographic and magnetic (electric) effects. However, the two-pass technique required twice more time for imaging. There are also other disadvantages, for example, a remote position of the probe during the second pass, which reduces a resolution and sensitivity of electric and magnetic imaging.

In past several years the interest to AFM-related modes for probing of electric and magnetic properties has increased due to improvements in EFM and Kelvin Force Microscopy. Kelvin Force Microscopy is method closely related to EFM but it provides quantitative measurements of surface potential. This is achieved by using an additional feedback mechanism, in which a voltage applied to the probe nullifies the effect of the contact potential difference (between the probe and the sample) on the oscillating probe. (In the tapping mode operation the KFM measurements are also can be done in the lift mode) In this way surface potential or surface charge can be measured quantitatively.

The increasing use of several lock-in amplifiers in the home-made and commercial scanning probe microscope allows researchers to perform topographic and electrostatic measurements in the single scan by operating the related signals and feedback loops at different frequencies. This approach has definite advantages compared to the two-pass mode: the improved sensitivity, higher resolution and a reduced experiment time.

Two-pass modes


EFM, SKPM
Probes with conducting coating
NSC18/Pt/AlBS


MFM
Probes with magnetic coating
NSC18/Co-Cr

 
 

 

 

 

 
 

OUR DISTRIBUTORS CONTACTS
MIKROMASCH
TOLL-FREE NUMBERS: USA: 1-866-SPMTIPS (776-8477)/ EU: + 8000-SPMTIPS (776-8477)
E-MAIL: INFO@MIKROMASCH.COM
RUS