Noncontact mode
|
 |
 |
 |
Options |
|
In noncontact mode, the long-distance van der Waals forces are
sensed by an oscillating probe, which is excited at its resonance
frequency by a piezoelectric transducer and brought in close proximity
to a sample. The probe oscillation amplitudes are typically in the
range of 1 nm or less. The resolution in this mode is defined by
the tip-sample separation of a few nanometers. For the scanning
feedback one can use ether the vibration amplitude (amplitude modulation
mode, AM) or the frequency shift (frequency modulation, FM) of the
probe.
|
 |
 |
 |
 |
 |
 |
 |
|
|
|
 |
| Fig.1 Microdrops of a liquid n-alkane
observed by AFM in non-contact mode. Image courtesy of A. Checco. |
 |
|
In Fig. 1, you can see an image of microdrops of a liquid n-alkane
on a silanized silicon substrate. The use of non-contact mode allowed
scanning without influencing the shape of the microdrops by tip-sample
forces.
To improve resolution in noncontact mode, one needs to enhance
sensitivity to short-range tip-sample forces. To do this, small
amplitudes of oscillation and small tip-sample distances are commonly
used. Advances in the development of the noncontact mode allow for
the discovery of single defects in atomic lattices. An image of
Si 7x7 surface obtained in noncontact mode is presented in Fig.2.
|
 |
 |
 |
 |
 |
 |
 |
|
|
|
 |
| Fig.2 AFM image of Si (111) 7x7 acquired
in noncontact mode on JEOL JSPM-4500A. |
 |
|
Operation at distances near the sample demands fine tip-force control
and the absence of surface contamination. That is why this technique
is mostly used in ultrahigh vacuum.
In most cases, the cantilever of choice for this mode is one with
a high spring constant between 20-100 N/m so that it does not stick
to the sample surface at small amplitudes. Between two cantilevers
having the same spring constant, it is better to use the one with
the higher resonant frequency. This lever is generally faster and
less noisy. Low-frequency cantilevers are used with AFM systems
that do not support probes with short lever arms.
Not surprisingly, imaging in noncontact mode is performed with
Si probes usually applied for tapping mode operation. It is likely
that in the near future, commercial AFM instruments will operate
in all oscillatory modes and the development of fast, broadband
controllers will lead to new multi frequency techniques. These techniques
might require the use of NanoTwist probes.
|
|
|
|
|





 |
MIKROMASCH
TOLL-FREE NUMBERS: USA: 1-866-SPMTIPS (776-8477)/ EU: + 8000-SPMTIPS (776-8477)
E-MAIL: INFO@MIKROMASCH.COM
|
RUS |
|