The ability of an AFM probe to profile sub-micron structures is
important for a number of technological applications in the semiconductor
and data storage industries. With the shrinking dimensions of semiconductor
and storage devices, it becomes more difficult to find suitable
techniques for quality control. Atomic force microscopy could potentially
be used for such a function, but its limitations have to be considered
for accurate application.
This issue is easily observed in studies of the surface roughness
of Si wafers and the porosity of low-K materials. As the sharpness
of the AFM tip increases, finer surface features can be revealed
which leads to a larger effective roughness estimated from height
images. This effect is illustrated by two images of a Si wafer,
one obtained with a regular (NSC 14) and the other obtained with
a DP14/Hi'RES probe. The two height images are compared below in
Figures 1a-b.
Fig.1. AFM images of a silicon wafer
surface from a conventional silicon etched probe (left) and a HI'RES
probe (right). Scan size µm. Dimension 5000 AFM. Images courtesy
of Dr. S. Magonov (Agilent).
larger than the roughness determined with the regular probe. Knowing
that there are large quantitative differences from using different
tips, it is important to clarify what type of data is necessary
for your application. If you need to qualitatively compare the roughness
of similar samples, a regular tip may be sufficient. However, if
you need accurate quantitative roughness data, it may be important
for you to use a Hi'Res tip for the best possible results.
It is worth noting that measurements taken with a sharp tip require
special precautions (a gentle engagement procedure and low-force
imaging) to avoid the unnecessary damage of the tip (see high-resolution
imaging for details).