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Diamond probe

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Application note

The new AFM probe for topography imaging is a single crystal diamond tip (see Fig. 1,2) mounted on silicon cantilever. The tip has a radius of about 7 nm and its cone angle is less than 20°, which allows imaging of high aspect ratio surface features and broadens the area for applications in comparison with silicon etched probes.

Fig.1. SEM photo of the diamond tip end Fig.2. SEM image of silicon cantilever and diamond probe tip

In Fig.3 you can see a comparison of scans made using the new diamond tip (a) and traditional silicon tip (c), with the corresponding height profiles. Scan 3a exhibits much higher profile as the tip can reach much deeper into the pores.

The tip exhibits high durability and resistance to wear. The scan 3a was made in contact mode, and inspite of the fact that the cone angle is less than 20°, it was not broken or weared off in this regime. A number of scans of rough and hard surface can be obtained by the same diamond tip even in contact mode without changing its shape, which is important for imaging different processes in time.

Comparison of AFM scans and height profiles of porous aluminum oxide made by diamond (a, b) and silicon (c, d) probes. Scan size 300 nm, height 60 nm (a) and 15 nm (c). The scale of the height profiles (b,d) is 80 nm. Scan (a) is made in contact mode, exhibiting the high durability of diamond tip.

The resolution attainable using the new diamond probes is comparable to that of silicon. Usual imaging procedures, techniques and AFM settings can be applied for scanning. An example of tapping mode scans made using diamond general purpose (GP) probes can be seen in Fig. 4.

 
Fig. 4
Tapping mode topography image of single molecules of fibrinogen on mica (Agilent 5500 AFM). Scan size 350x350 nm. Scan height 1.5 nm.

Image courtesy of S. Magonov, Agilent Technologies.
 
Product Specs

SCD probe is a single crystal Diamond tip mounted to the end of a silicon cantilever. The tip radius is about 7 nm, the aspect ratio is 4:1 or better.

         Detailed specifications »

Cantilever Resonant Frequency, kHz Force Constant, N/m
mintypicalmax mintypicalmax
Series 14 110 160 220 1.5 5.0 12.5
Series 15 250 300 350 20 40 75
Series 17 8.5 12 15 0.05 0.15 0.3
Series 18 75 100 125 2.0 3.5 5.5
Series 19 50 80 115 0.17 0.6 1.7
1-lever

325 kHz (46 N/m)

Series 15

160 kHz (5.0 N/m)

Series 14

75 kHz (3.5 N/m)

Series 18

80 kHz (0.63 N/m)

Series 19

12 kHz (0.15 N/m)

Series 17

 
 

 

 

 

 
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