The new AFM probe for topography imaging is a single crystal diamond
tip (see Fig. 1,2) mounted on silicon cantilever. The tip has a
radius of about 7 nm and its cone angle is less than 20°, which
allows imaging of high aspect ratio surface features and broadens
the area for applications in comparison with silicon etched probes.
Fig.1. SEM photo of the diamond tip end
Fig.2. SEM image of silicon cantilever
and diamond probe tip
In Fig.3 you can see a comparison of scans made using the new diamond
tip (a) and traditional silicon tip (c), with the corresponding
height profiles. Scan 3a exhibits much higher profile as the tip
can reach much deeper into the pores.
The tip exhibits high durability and resistance to wear. The scan
3a was made in contact mode, and inspite of the fact that the cone
angle is less than 20°, it was not broken or weared off in this
regime. A number of scans of rough and hard surface can be obtained
by the same diamond tip even in contact mode without changing its
shape, which is important for imaging different processes in time.
Comparison of AFM scans and height profiles of porous aluminum oxide made by diamond (a, b) and silicon (c, d) probes.
Scan size 300 nm, height 60 nm (a) and 15 nm (c). The scale of the height profiles (b,d) is 80 nm. Scan (a) is made in contact mode, exhibiting the high durability of diamond tip.
The resolution attainable using the new diamond probes is comparable
to that of silicon. Usual imaging procedures, techniques and AFM
settings can be applied for scanning. An example of tapping mode
scans made using diamond general purpose (GP) probes can be seen
in Fig. 4.
Fig. 4
Tapping mode topography image of single molecules of fibrinogen on
mica (Agilent 5500 AFM). Scan size 350x350 nm. Scan height 1.5 nm.
Image courtesy of S. Magonov, Agilent Technologies.
Product Specs
SCD probe is a single crystal Diamond tip mounted to the end of
a silicon cantilever. The tip radius is about 7 nm, the aspect ratio
is 4:1 or better.