SPM Probes   Materials Characterizing   TL series  

Application Note

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There are a number of AFM techniques sensitive to local mechanical properties of a sample. However, it is still challenging to distinguish between the different properties of materials like stiffness, hardness, adhesion, and viscoelasticity on these compositional maps.

The pioneering approach utilizes a probe with a T-shaped cantilever carrying a tip on one of its "wings". The offset of the tip from the cantilever longitudinal axis provides a very sensitive torsional response of the probe when the tip intermittently strikes a sample. A large number of harmonics are generated in the tip-sample contact that can be detected by broadband controllers.

Instead of imaging of any of detected harmonics, one can perform a conversion of harmonics data into time domain for reconstruction of tip-sample force curves practically in each oscillatory cycle of tip-sample interaction (Fig.1). Therefore, one can obtain topography information, phase image and map of any properties derived from the force curves (elastic modulus, adhesion, etc) in a single scan (Fig.2). Such a way provides unique extension of nanoindentation in low-force (10 pN), high-resolution (1 nm) and high-speed (10 sec) domains.

(a)(b)
Fig.1. Force-time and force-distance curves recorded in tapping mode on high-density PE layer (a) and low-density polyethylene layer (b).Image courtesy: Ozgur Sahin (The Rowland Institute at Harvard University).
(a) Height image.
(b) Phase image.
(c) Elastic modulus map (d) Elastic modulus map profile
Height, phase images and elastic modulus map of a multilayer polyethylene (PE) sample. Scan size 30 µ m. The contrast covers the height variations in the 0 - 100 nm scale in (a) and phase variations in the 0-30 degrees range in (b). (d) A profile of elastic modulus across the PE sample in the direction indicated with a white arrow in (c).
Image courtesy: Ozgur Sahin (The Rowland Institute at Harvard University).

Most samples that can be imaged in tapping mode in air can be investigated with TL300 probe. TL180 is for ultra high resolution mechanical measurements. This probe can perform sensitive mechanical measurements with peak tipsample forces less than 1 Nano Newtons as well as reliable and ultra-low force topographical imaging.

Product Specs

The nanoTWIST probe is a T-shaped cantilever having a tip on one of its arms. The positioning of the tip on one of the arms of the probe enhances its torsional motion when the tip interacts with the sample in the contact or oscillatory modes.

         Detailed specifications »

Cantilever Series Cantilever Length, l±5µm Cantilever Width, w±3µm Cantilever Thickness, µm Spring Constant, N/m Resonant Frequency, kHz Ftr/Ffl*
TL01 180 20 2.0 2.0 90 10±0.5
TL02 300 20 5.0 3.0 60 17±0.5
* Ratio of torsional to flexural resonance frequencies
TL-lever

90 kHz (Ftr/Ffl=10)

TL01

60 kHz (Ftr/Ffl=17)

TL02

 
 

 

 

 

 
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