Application Note
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There are a number of AFM techniques sensitive to local mechanical
properties of a sample. However, it is still challenging to distinguish
between the different properties of materials like stiffness, hardness,
adhesion, and viscoelasticity on these compositional maps.
The pioneering approach utilizes a probe with a T-shaped cantilever
carrying a tip on one of its "wings". The offset of the
tip from the cantilever longitudinal axis provides a very sensitive
torsional response of the probe when the tip intermittently strikes
a sample. A large number of harmonics are generated in the tip-sample
contact that can be detected by broadband controllers.
Instead of imaging of any of detected harmonics, one can perform
a conversion of harmonics data into time domain for reconstruction
of tip-sample force curves practically in each oscillatory cycle
of tip-sample interaction (Fig.1). Therefore, one can obtain topography
information, phase image and map of any properties derived from
the force curves (elastic modulus, adhesion, etc) in a single scan
(Fig.2). Such a way provides unique extension of nanoindentation
in low-force (10 pN), high-resolution (1 nm) and high-speed (10
sec) domains.
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(a) | (b) |
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| Fig.1. Force-time and force-distance
curves recorded in tapping mode on high-density PE layer (a) and low-density
polyethylene layer (b).Image courtesy: Ozgur Sahin (The Rowland Institute
at Harvard University). |
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| Cantilever Series |
Cantilever Length, l±5µm |
Cantilever Width, w±3µm |
Cantilever Thickness, µm |
Spring Constant, N/m |
Resonant Frequency, kHz |
Ftr/Ffl* |
| TL01 |
180 |
20 |
2.0 |
2.0 |
90 |
10±0.5 |
| TL02 |
300 |
20 |
5.0 |
3.0 |
60 |
17±0.5 |
* Ratio of torsional to flexural resonance frequencies
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